Preparation and performance test of an ultra-high temperature and acid resistant polymer
DOI:
CSTR:
Author:
Affiliation:

Clc Number:

TE357

Fund Project:

  • Article
  • |
  • Figures
  • |
  • Metrics
  • |
  • Reference
  • |
  • Related
  • |
  • Cited by
  • |
  • Materials
  • |
  • Comments
    Abstract:

    In order to solve the problem that conventional polymers cannot meet the technical requirements of acid fracturing in ultra-high temperature and deep wells, two polymers SY-1 and SY-2 were prepared by free radical polymerization using acrylamide(AM) 2-trimethylammonium ethyl methacrylate chloride (DMC)and AM DMC SMA ( octadecyl methacrylate ) as raw materials, and their structures were characterized and their properties were tested. The results showed that 720 cm-1in SY-2 infrared spectrum was the bending vibration absorption peak of—(CH2)n—, and the monomer was successfully grafted onto the polyacrylamide molecular chain. Thermogravimetric analysis showed that the weight loss ratio of SY-1 to 600?Cwas 98%, and that of SY-2 was 86%, and the thermal stability was improved. In 20% hydrochloric acid, the mass fraction of SY-2 is 0.8%: 180?C, 170s-1 rheological properties test, SY-2 shear end viscosity 56mPa?s, 90?C, 120?C, 150?C shear 1h, viscosity 83.6mPa?s, 43.5mPa?s, 27.8mPa?s, shear stability were 85.66%, 74.45%, 52.01%. At 180?C and 3 MPa, the static acid-rock reaction rate is 8.94 ? 10-5 (g/cm2 ? s), which is one order of magnitude lower than the conventional SY-1 reaction rate of 1.69 ? 10-4 (g/cm2 ? s). It has good compatibility with corrosion inhibitor and iron ion stabilizer to overcome the application bottleneck of high temperature acid fracturing technology.

    Reference
    Related
    Cited by
Get Citation
Related Videos

Share
Article Metrics
  • Abstract:
  • PDF:
  • HTML:
  • Cited by:
History
  • Received:September 11,2021
  • Revised:December 13,2021
  • Adopted:December 21,2021
  • Online: January 11,2022
  • Published:
Article QR Code